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Table 2 Measurement values of kimchi cabbage reference materials by the developed ID-LC/MS/MS method

From: Development of an isotope dilution liquid chromatography/tandem mass spectrometry method for the accurate determination of neonicotinoid pesticides, imidacloprid, clothianidin, and thiamethoxam in kimchi cabbage reference materials

 

Imidacloprid

Chlothianidin

Thiamethoxam

Period 1

   

Average values (mg/kg, n = 10)

0.860

0.524

0.787

Standard deviation (%)

0.51

0.40

0.46

Expanded uncertainty (mg/kg)

0.020

0.012

0.014

Period 2

   

Average values (mg/kg, n = 4)

0.837

0.514

0.774

Standard deviation (%)

0.31

0.27

0.37

Expanded uncertainty (mg/kg)

0.034

0.015

0.023