Table 7 1H NMR Peak assignments in CDCl3 solvent
Peak ID | 1H NMR Peak (ppm) | Assignment | Input to calculations given in Additional file 11 |
|---|---|---|---|
1 | 5.80 | R-CH=CH2 | A |
2 | 4.95 | R-CH=CH2 | B |
3 | 5.40 | R-CH=CH-CH3 | C |
4 | 4.70 | R-C(CH3)=CH2 | Not included |
5 | 3.65 | R-CH2-OH | D |
6 | ~ 2 | R-CH2-CH=CH2 | E |
7 | ~ 1.6 | H2O, R-CH=CH-CH3 | Not included |
8 | 1.25 | R-CH2-R’ | F |
9 | 0.90 | R-CH3 | G |
10 | 9.80 | R-CHO | H |
11 | 8.10 | Contamination from vial lid (formates) | Not applicable |