Table 3 Experimental results for the compound C25H25N8O4Cl, HCl
From: Mat-CHN software for drug substance titrations in discovery and development
Analytical determination | Method | Experimental results (%w/w) |
|---|---|---|
Water content | Karl Fischer | 0.80 |
Water content | Karl Fischer | 0.85 |
Butanol-1 | CPG-head space | 0.35 (3500 ppm) |
Chloride ion content | Ionic chromatography | 6.21(1) |
Chloride ion content | Ionic chromatography | 5.82(1) |
Chloride ion content | Ionic chromatography | 6.03(1) |
Des-chlorinated Impurity | HPLC | 0.3 |
Di-chlorinated Impurity | HPLC | 0.6 |
%C | Elemental analysis | 51.720 |
%H | Elemental analysis | 4.708 |
%N | Elemental analysis | 19.054 |