Parameters | Instrumental conditions |
---|---|
Instruments | Pekin Elmer Gas Chromatograph Clarus 680 and Pekin Elmer Mass Spectrometer Clarus SQ 8C |
Column | PekinElmer, Elite-5MS (column 30 m × 0.250 mm I.D. × 1 μm) (60–350°C) |
Carrier gas | Helium |
Oven temperature | Initial temperature at 80°C and initial hold for 2.00min Ramp 1: 10.0/min to 150°C, hold for 1.00min Ramp 2: 15.0/min to 250°C, hold for 10.00min |
Total run time | 26.6min |
Split ratio | 10:1 |
Injection vol | 2μl |
Ionization technique | Electron impact ionization |
Mass analyzer | Triple quadrupole analyzer |