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Table 2 Ion transitions and collision energy values of SNAP-8 and IS

From: Method development for acetyl octapeptide-3 analysis by liquid chromatography-tandem mass spectrometry

Analyte

Precursor ion [M + 2H]2+ (m/z)

Product ions (m/z)

Transition 1a (m/z)

CE1c (V)

Transition 2b (m/z)

CE2c (V)

Transition 3b (m/z)

CE3c (V)

Acetyloctapeptide-3 (SNAP-8)

538

102

− 30

84

− 48

144

− 25

Acetylhexapeptide-3 (IS)

445

102

− 39

84

− 55

144

− 30

  1. aQuantification ion
  2. bQualitative ions
  3. cCollision energy