Skip to main content

Table 4 Urine stability experiment (n = 3)

From: A new approach for urinary vanillylmandelic acid determination using eVol microextraction by packed sorbent coupled to liquid chromatography-tandem mass spectrometry

Concentration (μg/mL)

Room temperature (42 h)

3 freeze-thaw cycle (− 80 °C)

Long-term storage (− 80 °C, 56 days)

Deviation (%)

CV (%)

Deviation (%)

CV (%)

Deviation (%)

CV (%)

3.50

− 6.6

3.2

− 2.3

5.0

2.3

3.0

10.0

2.3

2.9

13.3

2.4

0.3

2.8

80.0

1.1

2.2

10.0

2.8

− 4.3

4.5