Validation parameters | Results |
---|---|
Regression coefficient | 0.998 |
Slope | 13583 |
Intercept | 10304x |
Linearity range (μg/ml) | 2–12 |
Intra-day precision (n = 3, RSD, %) | 0.15–0.77 |
Inter-day precision (n = 3, RSD, %) | 0.17–0.98 |
Repeatability (n = 3, RSD, %) | 1.66 |
Accuracy | 99.44–100.49 |
DL (μg) | 0.015 |
QL (μg) | 0.41 |
Ruggedness | |
Analysts I (n = 3, RSD, %) | 1.59 |
Analysts II (n = 3, RSD, %) | 1.27 |
Robustness | Robust |
Specificity | Specific |
In-house tablet assay | 98.85 ± 0.13 |