From: A 1H NMR method for the estimation of hydrogen content for all petroleum products
No. | Name of the compound | %H, by NMRa | %H, theoretical | %Rel Err | H at d1 = 5 s/10 s/40 s/60 s Scan = 16 |
---|---|---|---|---|---|
1 | 1,2,4-Trichlorobenzene, Spectrochem, 99.5 % | 1.51 | 1.67 | −9.58 | 1.32/1.4/1.66/1.67b |
2 | 1,2-Dichlorobenzene, Spectrochem, 99.5 % | 2.55 | 2.74 | −10.58 | 2.24/2.34/2.68/2.77b |
3 | Furfuraldehyde, freshly distilled | 3.90 | 4.20 | −7.14 | 3.42/3.54/4.00/4.20b |
4 | 2-Methylnaphthalene, Aldrich, 98 % | 6.94 | 7.09 | −2.11 | |
5 | Toluene, Merck, 99.8 % | 8.70 | 8.70 | 0.00 | |
6 | 4-(Decyloxy)benzoic acid, Aldrich, 98 % | 8.91 | 9.08 | −1.98 | |
7 | Tetralin, Merck, 98 % | 8.94 | 9.15 | −2.30 | 9.10/8.97/8.95/8.95c |
8 | Dioxane, Fluka, 99.99 % | 9.13 | 9.15 | −0.22 | |
9 | Ethylbenzene, Aldrich, 99 % | 8.84 | 9.49 | −6.85 | 8.37/8.52/9.16/9.47b |
10 | Mesitylene, Aldrich, >99 % | 10.18 | 10.06 | 1.19 | |
11 | Propylbenzene, Merck, >98 % | 10.09 | 10.06 | 0.30 | 9.73/9.97/10.12/10.12b |
12 | 2-(2-Ethoxyethoxy)ethanol, 98 % | 10.25 | 10.52 | −2.57 | |
13 | Octylphenol, Aldrich, 98 % | 10.51 | 10.75 | −2.23 | |
14 | Tricyclo[5.2.1.0]decane, Aldrich, 98 % | 10.90 | 11.84 | −7.94 | |
15 | 2,4-Dimethyl-1,3-pentadiene, Aldrich, 98 % | 12.46 | 12.58 | −0.95 | |
16 | 2,5-Dimethyl-2,4-hexadiene, Aldrich, >96 % | 13.15 | 12.81 | 2.65 | |
17 | 2-Ethylhexanol, Aldrich, 99 % | 13.85 | 13.93 | −0.57 | 14.60/13.86/13.87/13.88d |
18 | Pentylcyclohexane, Koch-Light Lab Ltd., >99 % | 14.55 | 14.29 | 1.82 | |
19 | 2,4,4-Trimethyl-1-pentene, Aldrich, 99 % | 14.00 | 14.37 | −2.59 | 14.30/14.20/14.05/14.07c |
20 | Pentacosane, Aldrich, 99 % | 15.00 | 14.86 | 0.95 | |
21 | Octadecane, Aldrich, 99 % | 15.25 | 15.05 | 1.33 | |
22 | Dodecane, Aldrich, >99 % | 15.44 | 15.39 | 0.32 | 16.64/15.77/15.41/15.41d |
23 | Decane, Aldrich, >99 % | 15.73 | 15.59 | 0.90 | |
24 | Nonane, Aldrich, >99 % | 15.89 | 15.72 | 1.02 | |
25 | 2,2,4-Trimethylpentane, SDH, >99 % | 16.01 | 15.88 | 0.82 | 16.30/16.08/16.03/16.03d |