From: Rapid ultra-performance liquid chromatography assay of losartan potassium in bulk and formulations
Value | |||||
---|---|---|---|---|---|
Column temperature, 15-ppm LOS | 39°C, area | 40°C, area | 41°C, area | %RE | %RSD |
1,672,455 | 1,675,725 | 1,674,952 | −0.097 for 39°C −0.095 for 41°C | 0.13 for 39°C 0.12 for 41°C | |
1,671,846 | 1,672,374 | 1,671,854 | |||
1,674,985 | 1,671,377 | 1,671,853 | |||
1,673,917 | 1,671,377 | 1,670,988 | |||
1,674,992 | 1,671,377 | 1,669,852 | |||
1,677,866 | 1,669,455 | 1,673,479 | |||
Wavelength, 15-ppm LOS | 243 nm, area | 245 nm, area | 247 nm, area | %RE | %RSD |
1,672,379 | 1,675,725 | 1,672,874 | −0.093 for 241 nm −0.090 for 245 nm | 0.13 for 241 nm 0.06 for 245 nm | |
1,671,895 | 1,672,374 | 1,671,893 | |||
1,674,813 | 1,671,377 | 1,671,623 | |||
1,673,739 | 1,671,898 | 1,672,098 | |||
1,674,385 | 1,670,491 | 1,671,254 | |||
1,677,930 | 1,669,455 | 1,669,695 |