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Table 4 Robustness data of SHH and MAP PGIs at LOD and LOQ concentrations

From: A selective and sensitive LC-MS/MS method for the simultaneous determination of twopotential genotoxic impurities in celecoxib

Parameter Actual Low High
Flow variation 0.7 0.63 0.77
Column oven temperature (°C) 40 38 42
SHH    
 %RSD at LOD 1.37 1.34 1.76
 %RSD at LOQ 1.42 1.78 2.04
MAP    
 %RSD at LOD 0.68 1.42 0.74
 %RSD at LOQ 2.14 1.63 1.91