Skip to main content

Table 3 The recovery data of SHH and MAP PGIs at three different concentrations

From: A selective and sensitive LC-MS/MS method for the simultaneous determination of twopotential genotoxic impurities in celecoxib

Parameter

SHH

MAP

Accuracy at LOQ level (n = 3)

  

 Amount added (ppm)

0.06

0.06

 Amount recovered (ppm)

0.057

0.059

 %recovery

95.3

98.6

 %RSD

1.95

1.84

Accuracy at 100% level (n = 3)

  

 Amount added (ppm)

1.5

1.5

 Amount recovered (ppm)

1.479

1.521

 %recovery

98.6

101.4

 %RSD

1.95

1.84

Accuracy at 150% level (n = 3)

  

 Amount added (ppm)

3.0

3.0

 Amount recovered (ppm)

3.102

3.108

 %recovery

103.4

103.6

 %RSD

1.21

1.44

  1. n, number of determinations.